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OilExpress 4
PerkinElmer OilExpress 4 User Manual
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OilE
xpress
4
Oil Condition Monitoring
Syste
m
User’s Guide
M
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Table of Contents
Default Chapter
3
Table of Contents
3
Introduction
5
About this Manual
6
Using this Guide
6
Conventions
7
Conventions Used in this Manual
7
Part Numbers
7
Notes, Warnings and Cautions
7
Oilexpress 4 Oil Condition Monitoring Systems
10
Introduction to Oil Analysis by Infrared Spectroscopy
11
Infrared Absorption
11
Degradation Products
12
Additive Depletion
12
Common Contaminants
13
Standard Methods for Lubricants Analysis by FT-IR
13
References
15
Analysis Methods Provided
16
Warnings and Safety Information
17
Overview
18
Oilexpress 4 System Safety Summary
19
General Safety
20
Electrical Safety
20
Mechanical Hazards
22
Environment
22
Use of Flammable Solvents and Samples
24
Material Safety Data Sheets
26
Overview of the Oilexpress 4 System
27
System Specifications
28
Liquid Autosampler
29
Connection Panel
30
Varispan Pipetting Arm and Versatips
30
System Liquid Container(S)
31
Labware Configurations
33
Sample Racks
34
Tip Boxes
38
Injection Station
40
Autosampler Safety Shield and Stop Button
42
Spectrometer Module
43
Spectrometer Sample Compartment
43
Sample Shuttle
44
Flow Cell
44
Liquid Presence Sensor
45
Connections on the Spectrometer
46
Fluid Control Module
48
Connections on the FCM
49
Waste Container
52
Spectrometer and FCM Mounting System
53
Ultrasonic Liquid Level Sensor Bar (Optional)
54
FT-IR-Only Analysis with the 96-Position Rack Type
54
Ultrasonic Height Sensing Errors Dialog
56
Oil Dilution
57
Overview of the FT-IR Analysis Procedure
58
Single-Spectrometer System
58
Dual-Spectrometer (DUO) System
62
Getting Started with Oilexpress 4
67
Overview
68
Starting Oilexpress 4 Software
69
The Oilexpress 4 Window
70
Oilexpress 4 On-Screen Help System
72
Sample Preparation
73
Priming the System
74
Defining the Sampling Heights
76
Saving Spectra, Exporting Spectra and Reporting
78
Exporting Spectra
78
Exporting Results
79
Reporting
80
Running an Analysis
81
Modifying Scan Settings
88
Absolute Virtual Instrument (AVI)
89
AVI Correction
89
AVI Calibration
90
System Validation
92
Control Samples
92
System Checks
93
Maintenance and Troubleshooting
95
Flow Cell Maintenance
96
Cleaning Using Oilexpress 4 Software
96
Removing and Installing the Flow Cell
97
Disassembling the Flow Cell for Deep Cleaning
103
Empty Cell Spectrum
105
Calibrating the Pathlength of the Flow Cell
109
Installing the Flow Cell / Injection Station Fluid Lines
114
Autosampler Maintenance
118
Daily Preventative Maintenance
118
Weekly Preventative Maintenance
119
Spectrometer Maintenance
121
Changing to a Single-Spectrometer System (DUO Systems Only)
122
Removing the Sample Shuttle
122
Installing the Sample Shuttle
124
Fluid Control Module Maintenance
126
Moving the System
127
Troubleshooting
128
Spares and Consumables
141
Appendices
145
Appendix 1: Decontamination
146
Appendix 2: WEEE Instructions for Perkinelmer Products
147
Appendix 3: Liquid Handling
148
Appendix 4: Fluid Path Materials
149
Index
150
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PerkinElmer OilExpress 4 Specifications
General
Brand
PerkinElmer
Model
OilExpress 4
Category
Laboratory Equipment
Language
English
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