ABB PGC5000 User Manual

892J009MNAE | DBDID | 11
3.4 Symptom – Excessive Noise
Possible Cause
Action(s)
Bad electrical connections
Check the signal cable connection and the bias voltage cable
connection.
Check the signal cable shield for fit. The fitting should be snug.
Verify connection between ground rod and ground.
Air Leak
Leak-check all of the fittings within the oven system to verify a leak-
free system.
Insufficient clearance for
the plasma electrode
The plasma O-ring on the plasma tube is designed to prevent this
issue. If the plasma electrode
appears to be too close to the
Swagelok
®
fitting, remove power from the analyzer and remove the
plasma tube from the top nut.
Install or replace the plasma O
-ring on the plasma tube and re-install
the plasma tube.
3.5 Symptom – Elevated baseline
Possible Cause
Action(s)
Poor carrier gas
Background signal is directly linked to the quality of gases being used.
UHP (ultra
-high purity) gases should always be used. If gas quality is
suspected, replace gas with new UHP quality gas.
When UHP gases
cannot be used, a scrubber will need to be installed
to remove excess levels of oxygen, water, and trace hydrocarbons.
Air Leak
An air leak in the chromatographic system can also cause an elevated
baseline. Verify that there are no air leaks in the
chromatographic
system.
3.6 Symptom – Baseline drift
Possible Cause
Action(s)
Poor pressure control
Pressure controls not providing a consistent, pulse free, flow rate to
the detector can cause detector drift.
Monitor the pressure gauges on the supply cylinder and measure the
flow out of the exhaust port over a one
-hour time period to insure
correct flow conditions.
Column bleed
Re-condition or replace the column.
Plasma cell leak
Initially, this may appear as column bleed, but the signal will
equilibrate as the oven reaches an isothermal temperature.
Reset the plasma cell in the Swagelok
®
fitting and tighten to leak-free.
Contamination or late-
eluting peaks
It is possible that there is a late-eluting peak or contamination that is
coming off the column several runs after it was introduced.
Alter the cycle time of the injection to see is the baseline drift changes
location.
If this is confirmed, install filters to eliminate the contamination.
Extend the
instrument cycle time to elute the material prior to the
next analysis.
3.7 Symptom – Spikes
Possible Cause
Action(s)
Loose connections
Verify that the signal cable is securely attached to the electrometer
and the BNC fitting on the collector shield.
Missing ground leads
Verify that the ground lead from the plasma center electrode is
connected. If it is not, power the analyzer down and re
-connect the
center electrode ground lead.
Verify that the main power supply ground lead is connected to the
appropriate oven chassis ground point.

ABB PGC5000 Specifications

General

Brand	ABB
Model	PGC5000
Category	Laboratory Equipment
Language	English