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aanalyst 200
PerkinElmer aanalyst 200 User Manual
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AAnalyst 200
User’s Guide
2
Table of Contents
Default Chapter
3
Table of Contents
3
Chapter 1 Introduction
7
About this Manual
9
Conventions Used in this Manual
11
Warning Labels on the Instrument
12
Chapter 2 Safety Practices
19
Chapter Overview
21
Working Safely with the Aanalyst 200
22
Precautions
23
Hazards with Flame Atomization
24
Safety Conventions in the Hardware Guide
26
Symbols Used on the Instrument
27
Safety Practices for Flame Atomization
28
High Temperatures
30
Electrical Safety
31
Compressed Gases
32
Safe Handling of Gas Cylinders
33
Operating Conditions
36
Exhaust Venting
37
Safe Handling of Chemicals
38
Decontamination
39
Waste Disposal
40
Electromagnetic Compatibility (EMC)
41
WEEE Instructions for Perkinelmer Products
42
References for Laboratory Safety Practice
43
Chapter 3 Preparing Your Laboratory
47
Introduction
47
Environmental Conditions
48
General Laboratory Requirements
49
Location and Space Requirements
51
Exhaust Vent Requirements
56
Electrical Requirements
64
Lamps
65
Chapter 4 System Description
67
Introduction
69
Aanalyst 200 Overview
70
The Aanalyst 200 Spectrometer System
71
General Lamp Information
72
The Deuterium Arc Background Corrector
77
The Burner System
78
Connecting the Electrical Supply
85
Mercury/Hydride Determination System (MHS-15)
87
Chapter 5 Installation
89
Introduction to the Installation Procedure
91
When the Spectrometer Arrives
92
Placing the Spectrometer on the Bench
94
Aanalyst 200 Shipping List
96
Aanalyst 200 Spares Kit
97
Installing the Touch Screen
98
Connecting the Gas Hoses
102
Setting up the Burner System
107
Installing the Burner Door
109
Installing the Sample Tray
110
Connecting to the Electrical Supply
111
Switches and Connectors on the E-Box
112
Setting up the Autosampler
113
Connecting the Foot Switch
114
Chapter 6 Operation of Instrument
117
Starting up the System
117
Setting up the Burner System
119
Installing Solvent-Resistant Components in the Burner
125
User Interface
133
Installing Lamps
135
Switching on the Spectrometer
139
Safety Checks
140
Using the Background Corrector
141
Optimization Procedures
142
Aligning Lamp
143
Setting the Burner Height
147
Igniting the Flame
149
Preadjusting the Nebulizer
151
Optimizing the Burner System
153
Rinsing the Burner System
157
Chapter 7 Touch Screen
161
User Interface
161
Startup Dialog
163
Lamp Page
164
Flame Page
169
Parameters Page
172
Analyze Page: Manual Data Display
178
Analyze Samples Page: Manual Continuous Display
181
Analyze Page: Autosampler
183
Tools Dialog
185
Recommended Conditions
189
Network Dialog
190
Download
199
Importing Aanalyst 200 into Microsoft Excel
205
Chapter 8 Analyzing Samples
211
Sequence of Operations
213
Manual Flame Analyses
214
Automated Flame Analyses
225
Manual Analyses: Data Display MHS-Technique
232
Running Samples in Emission Mode
233
Shutting down the System
241
Emergency Shutdown
242
Rinsing the Burner System
243
Chapter 9 Maintenance
245
Introduction
247
General Maintenance Checklist
248
Instrument Maintenance Checklist
249
Checks
251
Spectrometer Maintenance Checklists
252
Burner Maintenance Checklist
253
Changing the Air Filter
255
Extinguishing the Flame
256
Cleaning the Burner Chamber
257
Removing the Burner Door
259
Replacing the Burner Door
260
Cleaning the Burner System
261
Cleaning the Burner Head
263
Pre-Conditioning a New Burner or Drain Tube
265
Removing the Burner Head
266
Removing the Burner Assembly from the Instrument
267
Disassembling the Burner Chamber
269
Reassembling the Burner System
272
Drain System Maintenance
276
Cleaning the Nebulizer
280
Replacing Parts of Wear
289
E-Box
290
Maintaining the Acetylene Supply
294
Replacing the Lamps
295
Replacing the Deuterium Arc Background Corrector Lamp
296
AS-90Plus and AS-93Plus Autosampler Maintenance
300
MHS-15 Mercury/Hydride System Maintenance
301
Replacement Parts and Accessories
304
Chapter 10 Troubleshooting
307
Introduction
309
Flame Analysis Troubleshooting
310
Flame/Burner Troubleshooting
314
Lamp Troubleshooting
317
Troubleshooting Deuterium Background Corrector Problems
319
Index
321
4
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PerkinElmer aanalyst 200 Specifications
General
Brand
PerkinElmer
Model
aanalyst 200
Category
Laboratory Equipment
Language
English
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