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CLARUS SQ 8 MS
PerkinElmer CLARUS SQ 8 MS User Manual
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C
LARUS
SQ 8 MS
Hardware Guide
GAS CHROMATOGRAPHY
2
Table of Contents
Default Chapter
5
Table of Contents
5
Warnings and Safety Information
9
Conventions Used in this Manual
11
Customer Service
14
Electromagnetic Compatibility (EMC)
15
Europe
15
South Korea
15
United States (FCC)
16
Electrical Symbols Used on Clarus SQ 8 MS Series
17
Label Location and Content
18
Clarus MS Safety Practices
21
Generic Warnings
21
Moving the Clarus SQ 8 MS
21
Electrical High Voltage
22
Contamination
26
Decontamination
27
Cleaning the Instrument
27
General Laboratory Safety
28
Compressed Gases
28
Ventilation
29
Heated Zones
30
Using Hydrogen, Methane or Isobutane
30
Using Ammonia Gas
31
Hazardous Chemicals
32
Definitions in Warning for Hazardous Chemicals
34
Temperature, Humidity, and Environment
35
Operating Conditions
35
Storage Conditions
37
General Laboratory Safety
37
Cleaning Requirements
37
WEEE Instructions for Perkinelmer Products
38
Pre-Installation Requirements
39
Laboratory Space Requirements
39
Environmental Requirements
40
Power Requirements
41
Gas Requirements
42
Safety Requirements
43
Pre-Installation Checklist
45
Introduction
47
Preface
49
System Overview
49
Summary of this Guide
50
Related Documentation
50
Supplies, Accessories and Replacement Parts
51
About the Clarus GC/MS System
53
About the Clarus SQ 8 MS System
55
Clarus 580/680 Series GC
57
GC Interface (Transfer Line)
58
Reference Gas Inlet
58
Ion Optics Path
59
Vacuum System
60
Rotary Pump
60
Vacuum Pump Options
61
Turbomass Software
63
Top Level Screen
63
Tune Page
63
Analytical Column
65
Pre-Operational Checklist
66
Maintenance
67
Overview
70
Typical Overall Maintenance Schedule
73
Daily
73
Weekly
73
Monthly
74
Every Six Months
74
Yearly
74
Leak Checking
75
Tuning the Clarus MS
78
Preparing Clarus MS for Hardware Maintenance
80
Removing and Returning the Source
84
Removing the Source
84
Returning the Source
88
Changing a Column
90
Tools and Items Required
90
Physical Measurement Outside the SQ 8MS
92
Alignment Using the 10 MM Positioning Gauge Tool
95
Optical Column Alignment Using the Optional Plug Handle and Sight
97
Refilling the Reference Gas Vial
102
Items Required
102
Replacing a Filament
105
Items and Tools Required
105
Source Maintenance
110
Mass Analyzer Maintenance (Perkinelmer Service Representative Only)
115
Items and Tools Required
115
Cleaning Materials
116
Removing and Returning the Ion Optics Assembly
117
Replacing the Electron Multiplier
127
Cleaning the Prequads
128
Changing to CI
138
Leak Checking
139
Setting-Up CI
141
Troubleshooting
148
Overview
150
Spare Components
151
Logical Troubleshooting Steps
151
Troubleshooting Chart
153
Chromatography Related
164
Spectral Related
168
Communications Related
170
Forepump Related
171
Message Dialogs
174
Index
179
4
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PerkinElmer CLARUS SQ 8 MS Specifications
General
Brand
PerkinElmer
Model
CLARUS SQ 8 MS
Category
Laboratory Equipment
Language
English
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