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CLARUS 680 GC
PerkinElmer CLARUS 680 GC User Manual
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C
LARUS
600/680 GC
User’s Guide
GAS CHROMATOGRAPHY
2
Table of Contents
Default Chapter
5
Table of Contents
5
Introduction
11
About this Manual
13
Conventions Used in this Manual
14
Notes, Cautions and Warnings
14
Warning Signs on the Instrument
15
Screen Abbreviations
16
Glossary of Clarus GC Terms
17
Autosampler Terms
17
Instrument-Specific Terms
18
Glossary of Chromatographic Terms
20
Touch Screen Navigation
23
Chapter Overview
25
Touch Screen
26
Tabs
28
Non-Configured Devices
28
Non-Installed Devices
29
Run Button
30
Stop Menu
33
Signal Button
33
Heated Zones
35
Navigation Bar
38
Injectors
39
Program Buttons
40
Display Text
40
Pss
40
Packed (Pkd)
46
Poc
50
Capillary (Cap) Injector
51
Oven
52
Aux Zone
53
Detectors
54
Fid
54
Tcd
58
Ecd
59
Pid
61
Npd
62
Fpd
63
Timed Events
64
Events Tab
64
Timed Events Table
65
Using the Active Method
73
Overview
75
Editing the Active Method
76
Getting Ready to Edit the Active Method
77
Setting up Oven and Inlet Temperature Programs
78
Configuring the Equilibration Time (Init)
79
Setting a Coolant Timeout Value
79
Setting a Coolant Cut-In Temperature
80
Setting up an Isothermal Program
80
Setting up a One-Ramp Temperature Program
82
Holding an Oven Temperature
83
Setting Injector Temperatures
86
Displaying Injector Temperature Screens
86
Turning Injector Heaters on or off
88
Changing Injector Temperatures
88
Oven Temperature Programming Mode
89
Inlet Temperature Programming Mode
90
Setting up a One-Ramp Injector Program
91
Viewing/Setting Carrier Gas Pressure/Flow/Velocity
93
Setting Carrier Gas Pressure
95
Setting Carrier Gas Flow Using PPC
97
Viewing/Setting Carrier Gas Velocity
99
Setting the Septum Purge Mode and Offset
101
Setting up Valves
109
Setting the Split Mode Using PPC
109
Set up the Splitless Mode for a CAP or PSS Injector
113
Splitless Injection with Pressure Pulse (Flow Pulse, Velocity Pulse) Technique
113
Contolling the Autosampler
123
Autosampler Trays and Carousel
123
Autosampler Touch Screen
125
Start Button
126
Stop Button
127
About Waste and Wash Vials
134
Multi-Program Mode
134
About Sample Vials
135
Using a TCD with the Autosampler
135
Available Syringes
136
Setting up the Detectors
137
Overview
139
FID Overview
141
Setting up an FID
142
Automatically Ignite the Flame
147
Manually Ignite the Flame
149
Using the FID in Corrosive Environments
151
Setting up an ECD
153
United States Government Regulations for Ecds
153
Special Instructions for ECD Cell Purchasers
154
United Kingdom Regulations
156
ECD Overview
156
ECD Set up
158
Setting up a TCD
164
TCD Setup
165
TCD Setup Summary
165
Using a TCD with the Autosampler or GSV
171
Setting up a PID
172
PID Overview
172
PID Setup
173
Setting up a NPD
179
NPD Overview
180
Setting up a NPD
181
NPD Bead Activation Procedure
184
Setting up an FPD
191
FPD Overview
191
Setting up the FPD
193
FPD Setup Summary
193
Configure the Linearizer and Signal Filter
193
Set the FPD Temperature
197
Detector Temperatures
208
Setting the Range
210
Setting the FID, PID, or NPD Range
210
Changing the FID, PID, or NPD Range During a Run
211
Setting the TCD Current (Filament Current)
214
Changing TCD Polarity During a Run
216
Routing Detector Output
219
Rerouting Output
219
Attenuating Detector Signals Going to a Recorder
223
Optimizing a Detector Signal to an Integrator for Maximum Sample Dynamic Range
225
Matching Detector Signals with Your Integrator
226
Autozeroing a Detector
229
Using the Method Editor
231
Method Editor
233
Method Edit Mode
235
Oven Settings
237
Managing Methods
239
File Menu
239
Using the Tools Menu
249
Tools Menu
251
Method Editor
252
Event Log
253
Maintenance
254
Configuration
258
Injectors (Deconfiguring and Configuring Injectors)
258
Oven
266
Detectors
268
Run/Autosampler
274
Setup
276
Pneumatics
281
Connecting the PPC Modules
283
Reference Settings
296
Relays
296
Zeroing and Calibrating the PPC Modules
297
Zeroing the PPC Gas Modules
297
Setting the Reference Temperature and Pressure
301
Calibrating the Carrier Gas Modules
302
Calibrating the Detector Gas Modules
305
Calibrating the Oven Temperature
308
Calibrate the Reference Thermometer
308
Place the Thermometer Probe in the Oven
309
Equilibrate the Oven Temperature
310
Enter the Required Offset Value
313
Remove the Thermometer Probe
313
Utilities
314
Column Flow Calculator
315
Split Flow Calculations Screen
319
Column Length Calculator
321
Background Compensation
322
Stopwatch
324
Program (Max Oven Program Rates)
325
Release
326
Logout
327
About
328
Setting up a Typical Analysis
329
System Status Screen
332
Injector Settings
334
Packed Column (PKD) Injector
334
Programmed Split/Splitless (PSS) Injector
336
Detector Settings
339
Flame Ionization Detector (FID)
339
Detector
344
Thermal Conductivity Detector (TCD)
344
Autosampler
350
Index
355
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PerkinElmer CLARUS 680 GC Specifications
General
Brand
PerkinElmer
Model
CLARUS 680 GC
Category
Laboratory Equipment
Language
English
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