List of Figures
H155936_3_003
57
List of Figures
Figure 4.1: InsightMR Flow Tube Assembly and the Transfer Line ................................................ 15
Figure 4.2: Recommended Laboratory Setup................................................................................. 16
Figure 4.3: InsightMR Flow Tube Assembly, Flow Tube Protector and Flow Interface .................. 17
Figure 6.1: Typical Laboratory Setup for Monitoring Chemical Reaction........................................ 23
Figure 6.2: The Transfer Line Holder.............................................................................................. 24
Figure 6.3: The InsightMR Flow Unit. From left to right: the pump, the reactor, the flow tube as-
sembly secured with a clamp stand and the thermostat............................................... 24
Figure 6.4: From Left to Right, Glass Flow Tube O-Rings, Vessel Connections ,and Flow Inter-
face Valve ..................................................................................................................... 25
Figure 6.5: Temperature Control Connections................................................................................ 26
Figure 6.6: The TopSpin Setup Tool............................................................................................... 28
Figure 6.7: Selection of Components to Install ............................................................................... 28
Figure 6.8: TopSpin Release Letter Confirmation........................................................................... 28
Figure 6.9: Select an Installation Directory ..................................................................................... 29
Figure 6.10: Warning Message when the Installation Directory does not Exist ................................ 29
Figure 6.11: Select Setup Type ........................................................................................................ 29
Figure 6.12: Select Products to Install .............................................................................................. 30
Figure 6.13: Select the NMR Super User ......................................................................................... 30
Figure 6.14: Select an NMR Administration Password ..................................................................... 31
Figure 6.15: Installation Finished ...................................................................................................... 31
Figure 6.16: InsightMR Release Letter ............................................................................................. 31
Figure 6.17: Configuration Check ..................................................................................................... 32
Figure 6.18: InsightMR Icon.............................................................................................................. 32
Figure 6.19: Starting the Icon Configuration ..................................................................................... 33
Figure 6.20: IconNMR Configuration - Resource File Settings ......................................................... 33
Figure 6.21: Restoring the Default Settings ...................................................................................... 34
Figure 6.22: Configuring the Master Switches .................................................................................. 34
Figure 6.23: Configuring the Automation Window ............................................................................ 35
Figure 6.24: Selecting the Solvent and Probe Dependencies .......................................................... 35
Figure 6.25: Selecting the Tuning and Matching Options ................................................................. 36
Figure 6.26: InsightMR Acquisition Window Expansion Showing the New Protonated Solvents ..... 36
Figure 6.27: Edsolv in TopSpin......................................................................................................... 37
Figure 6.28: Solvents in the IconNMR Configuration........................................................................ 37
Figure 7.1: Inserting the Flow Unit Assembly into the Magnet........................................................ 39
Figure 7.2: Mounting the Insulated Transfer Line ........................................................................... 40
Figure 7.3: The Unhook Button....................................................................................................... 41
Figure 8.1: InsightMR Flow Unit Laboratory Setup ......................................................................... 43
Figure 9.1: InsightMR Flow Unit Laboratory Setup ......................................................................... 47
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